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In arid regions, flash floods often occur as a consequence of excessive rainfall. Occasionally causing major loss of property and life, floods are large events of relatively short duration. Makkah area in western Saudi Arabia is characterized by high rainfall intensity that leads to flash floods. This study quantifies the hydrological characteristics and flood probability of some major wadis in western Saudi Arabia, including Na’man, Fatimah, and Usfan. Flood responses in these wadis vary due to the nature and rainfall distribution within these wadis. Rainfall frequency analysis was performed using selected annual maximums of 24-h rainfall from eight stations located in the area. Two of the most applied methods of statistical distribution, Gumbel’s extreme value distribution and log Pearson type III distribution, were applied to maximum daily rainfall data over 26 to 40 years. The Gumbel’s model was found to be the best fitting model for identifying and predicting future rainfall occurrence. Rainfall estimations from different return periods were identified. Probable maximum floods of the major wadis studied were also estimated for different return periods, which were extrapolated from the probable maximum precipitation.