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DOI10.19756/j.issn.0253-3820.221346
Rapid Detection of 17 Kinds of Perfluoroalkyl Substances in Drinking Water by Solid phase Extraction-Liquid Chromatography-Tandem Mass Spectrometry Based on Metal Organic Frameworks DUT 5-2
Wu, Feng; Hu, Yue; Guo, Meng-Meng; Song, Zhi-Ling; Tan, Zhi-Jun; Geng, Qian-Qian
通讯作者Guo, MM
来源期刊CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
ISSN0253-3820
EISSN1872-2040
出版年2023
卷号51期号:9页码:1506-1517
英文摘要A method was developed for rapid detection of 17 kinds of perfluoroalkyl substances (PFAS) in drinking water by self-made solid phase extraction (SPE) column using metal-organic frameworks DUT-5-2 as adsorbent coupled with liquid chromatography-quadrupole/linear ion trap tandem mass spectrometry. The calibration curves were linear well with correlation coefficients cover 0.995. The limits of detection were 0.8-8.0 ng/L. The limits of quantification were 2.5-25.0 ng/L. The average spiked recoveries for 17 kinds of PFAS were 62.9%-119.9%, with relative standard derivations (RSDs) of 0.1%-14.8%. This method showed many advantages such as rapidity, economy, high sensitivity, accuracy and precision compared with commercial Oasis HLB and Oasis WAX SPE columns-based methods. The recoveries of the method still met the detection requirements after 4 cycles of regeneration, and was suitable for detection of actual drinking water samples. This method provided an efficient analytical tool for monitoring PFAS pollution in drinking water.
英文关键词Metal-organic frameworks Rapid detection Perfluoroalkyl substances Solid phase extraction-liquid chromatography-mass spectrometry Drinking water
类型Article
语种中文
收录类别SCI-E
WOS记录号WOS:001092287600001
WOS类目Chemistry, Analytical
WOS研究方向Chemistry
资源类型期刊论文
条目标识符http://119.78.100.177/qdio/handle/2XILL650/395754
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Wu, Feng,Hu, Yue,Guo, Meng-Meng,et al. Rapid Detection of 17 Kinds of Perfluoroalkyl Substances in Drinking Water by Solid phase Extraction-Liquid Chromatography-Tandem Mass Spectrometry Based on Metal Organic Frameworks DUT 5-2[J],2023,51(9):1506-1517.
APA Wu, Feng,Hu, Yue,Guo, Meng-Meng,Song, Zhi-Ling,Tan, Zhi-Jun,&Geng, Qian-Qian.(2023).Rapid Detection of 17 Kinds of Perfluoroalkyl Substances in Drinking Water by Solid phase Extraction-Liquid Chromatography-Tandem Mass Spectrometry Based on Metal Organic Frameworks DUT 5-2.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,51(9),1506-1517.
MLA Wu, Feng,et al."Rapid Detection of 17 Kinds of Perfluoroalkyl Substances in Drinking Water by Solid phase Extraction-Liquid Chromatography-Tandem Mass Spectrometry Based on Metal Organic Frameworks DUT 5-2".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 51.9(2023):1506-1517.
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