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DOI	10.1039/d2ay01807a
	Efficient determination of non-steroidal anti-inflammatory drugs by micellar electrokinetic chromatography in wastewater
	Alatawi, Hanan; Hogan, Anna; Albalawi, Ibtihaj; Alsefri, Samia; Moore, Eric
通讯作者	Moore, E
来源期刊	ANALYTICAL METHODS
ISSN	1759-9660
EISSN	1759-9679
出版年	2023
卷号	15 期号:11 页码:1402-1409
英文摘要	Recently, non-steroidal anti-inflammatory drugs (NSAIDs) have been increasingly used in humans and animals. Despite being effective against a wide variety of diseases, they pose a threat to aquatic environments. In the current work, a highly efficient, selective, and sensitive micellar electrokinetic chromatography (MEKC) method was developed for the determination of five NSAIDs in environmental water samples. The optimal separation BGE was 15 mM borate buffer (pH 9), 90 mM SDS, and 10% methanol at a separation voltage of 15 kV and a hydrodynamic injection of 10 mbar for 5 s. The results presented in this study provide a higher number of theoretical plates N > 780 000 with excellent RSDs of 0.1-1.5% and great sensitivity (3-15 mu g L-1) for NSAIDs. To validate this method, the solid phase extraction method was optimized using two different cartridges (C18 and Oasis HLB); the results showed excellent recoveries (73-111.6%) for all the analytes in wastewater samples.
类型	Article
语种	英语
开放获取类型	Green Published, hybrid
收录类别	SCI-E
WOS记录号	WOS:000916750200001
WOS关键词	SOLID-PHASE EXTRACTION ; CAPILLARY-ZONE-ELECTROPHORESIS ; PERSONAL-CARE PRODUCTS ; ACETYLSALICYLIC-ACID ; SEPARATION ; PHARMACEUTICALS ; PRECONCENTRATION ; IBUPROFEN ; STRENGTH ; NAPROXEN
WOS类目	Chemistry, Analytical ; Food Science & Technology ; Spectroscopy
WOS研究方向	Chemistry ; Food Science & Technology ; Spectroscopy
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/395294
推荐引用方式 GB/T 7714	Alatawi, Hanan,Hogan, Anna,Albalawi, Ibtihaj,et al. Efficient determination of non-steroidal anti-inflammatory drugs by micellar electrokinetic chromatography in wastewater[J],2023,15(11):1402-1409.
APA	Alatawi, Hanan,Hogan, Anna,Albalawi, Ibtihaj,Alsefri, Samia,&Moore, Eric.(2023).Efficient determination of non-steroidal anti-inflammatory drugs by micellar electrokinetic chromatography in wastewater.ANALYTICAL METHODS,15(11),1402-1409.
MLA	Alatawi, Hanan,et al."Efficient determination of non-steroidal anti-inflammatory drugs by micellar electrokinetic chromatography in wastewater".ANALYTICAL METHODS 15.11(2023):1402-1409.