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DOI10.1016/j.foodchem.2022.133260
Simultaneous screening and analysis of 155 veterinary drugs in livestock foods using ultra-high performance liquid chromatography tandem quadrupole linear-ion-trap mass spectrometry
Wang, Juanqiang; Zhao, Wentao; Guo, Wenping; Li, Yingying; Jiang, Rui; Li, Huichen; Wang, Shouwei; Li, Zhigang
通讯作者Wang, SW
来源期刊FOOD CHEMISTRY
ISSN0308-8146
EISSN1873-7072
出版年2022
卷号393
英文摘要Veterinary drugs are widely used to improve the health and growth of livestock. The supervision of these residues is necessary to ensure food safety. A high-throughput method based on Oasis PRiME HLB with solid phase extraction for simultaneous qualitative and quantitative analysis of 155 veterinary drugs in livestock foods was developed by the ultra-high performance liquid chromatography tandem quadrupole linear-ion-trap mass spectrometry (UHPLC-QTRAP-MS). The limits of detection and quantification ranged from 0.5 mu g/kg to 5 mu g/kg and 2 mu g/kg to 20 mu g/kg, respectively. For over 85% of the analytes, the recoveries were between 60% and 120%. The positive simulated samples perfectly matched with a purity fit value over 70% from the self-built library. The screening results of UHPLC-QTRAP-MS were almost consistent with UHPLC tandem quadrupole-exactive orbitrap mass spectrometry (UHPLC-Q-Exactive Orbitrap/MS). The evaluated UHPLC-QTRAP-MS method was powerful and reliable for the screening and quantification of veterinary drugs in real samples.
英文关键词Multi-residue analysis Livestock foods Ultra-high performance liquid chromatography tandemquadrupole linear-ion-trap mass spec-trometry Veterinary drugs Qualitative screening Quantitative analysis
类型Article
语种英语
收录类别SCI-E
WOS记录号WOS:000823309000012
WOS关键词QUANTITATIVE-ANALYSIS ; PESTICIDES ; RESIDUES ; MYCOTOXINS
WOS类目Chemistry, Applied ; Food Science & Technology ; Nutrition & Dietetics
WOS研究方向Chemistry ; Food Science & Technology ; Nutrition & Dietetics
资源类型期刊论文
条目标识符http://119.78.100.177/qdio/handle/2XILL650/392595
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Wang, Juanqiang,Zhao, Wentao,Guo, Wenping,et al. Simultaneous screening and analysis of 155 veterinary drugs in livestock foods using ultra-high performance liquid chromatography tandem quadrupole linear-ion-trap mass spectrometry[J],2022,393.
APA Wang, Juanqiang.,Zhao, Wentao.,Guo, Wenping.,Li, Yingying.,Jiang, Rui.,...&Li, Zhigang.(2022).Simultaneous screening and analysis of 155 veterinary drugs in livestock foods using ultra-high performance liquid chromatography tandem quadrupole linear-ion-trap mass spectrometry.FOOD CHEMISTRY,393.
MLA Wang, Juanqiang,et al."Simultaneous screening and analysis of 155 veterinary drugs in livestock foods using ultra-high performance liquid chromatography tandem quadrupole linear-ion-trap mass spectrometry".FOOD CHEMISTRY 393(2022).
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