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DOI | 10.1016/j.foodchem.2022.133260 |
Simultaneous screening and analysis of 155 veterinary drugs in livestock foods using ultra-high performance liquid chromatography tandem quadrupole linear-ion-trap mass spectrometry | |
Wang, Juanqiang; Zhao, Wentao; Guo, Wenping; Li, Yingying; Jiang, Rui; Li, Huichen; Wang, Shouwei; Li, Zhigang | |
通讯作者 | Wang, SW |
来源期刊 | FOOD CHEMISTRY
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ISSN | 0308-8146 |
EISSN | 1873-7072 |
出版年 | 2022 |
卷号 | 393 |
英文摘要 | Veterinary drugs are widely used to improve the health and growth of livestock. The supervision of these residues is necessary to ensure food safety. A high-throughput method based on Oasis PRiME HLB with solid phase extraction for simultaneous qualitative and quantitative analysis of 155 veterinary drugs in livestock foods was developed by the ultra-high performance liquid chromatography tandem quadrupole linear-ion-trap mass spectrometry (UHPLC-QTRAP-MS). The limits of detection and quantification ranged from 0.5 mu g/kg to 5 mu g/kg and 2 mu g/kg to 20 mu g/kg, respectively. For over 85% of the analytes, the recoveries were between 60% and 120%. The positive simulated samples perfectly matched with a purity fit value over 70% from the self-built library. The screening results of UHPLC-QTRAP-MS were almost consistent with UHPLC tandem quadrupole-exactive orbitrap mass spectrometry (UHPLC-Q-Exactive Orbitrap/MS). The evaluated UHPLC-QTRAP-MS method was powerful and reliable for the screening and quantification of veterinary drugs in real samples. |
英文关键词 | Multi-residue analysis Livestock foods Ultra-high performance liquid chromatography tandemquadrupole linear-ion-trap mass spec-trometry Veterinary drugs Qualitative screening Quantitative analysis |
类型 | Article |
语种 | 英语 |
收录类别 | SCI-E |
WOS记录号 | WOS:000823309000012 |
WOS关键词 | QUANTITATIVE-ANALYSIS ; PESTICIDES ; RESIDUES ; MYCOTOXINS |
WOS类目 | Chemistry, Applied ; Food Science & Technology ; Nutrition & Dietetics |
WOS研究方向 | Chemistry ; Food Science & Technology ; Nutrition & Dietetics |
资源类型 | 期刊论文 |
条目标识符 | http://119.78.100.177/qdio/handle/2XILL650/392595 |
推荐引用方式 GB/T 7714 | Wang, Juanqiang,Zhao, Wentao,Guo, Wenping,et al. Simultaneous screening and analysis of 155 veterinary drugs in livestock foods using ultra-high performance liquid chromatography tandem quadrupole linear-ion-trap mass spectrometry[J],2022,393. |
APA | Wang, Juanqiang.,Zhao, Wentao.,Guo, Wenping.,Li, Yingying.,Jiang, Rui.,...&Li, Zhigang.(2022).Simultaneous screening and analysis of 155 veterinary drugs in livestock foods using ultra-high performance liquid chromatography tandem quadrupole linear-ion-trap mass spectrometry.FOOD CHEMISTRY,393. |
MLA | Wang, Juanqiang,et al."Simultaneous screening and analysis of 155 veterinary drugs in livestock foods using ultra-high performance liquid chromatography tandem quadrupole linear-ion-trap mass spectrometry".FOOD CHEMISTRY 393(2022). |
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