干旱区生态环境知识资源中心(Arid): Determination of Caffeine, Theobromine, and Theophylline in Chocolate Using LC-MS

Arid

	Determination of Caffeine, Theobromine, and Theophylline in Chocolate Using LC-MS
	Tanaka, Tomoya; Kimura, Keisuke; Kan, Kimiko; Shindo, Tetsuya; Sasamoto, Takeo
通讯作者	Tanaka, T (corresponding author), Tokyo Metropolitan Inst Publ Hlth, Shinjuku Ku, 3-24-1 Hyakunin Cho, Tokyo 1690073, Japan.
来源期刊	FOOD HYGIENE AND SAFETY SCIENCE
ISSN	0015-6426
出版年	2021
卷号	62 期号:4 页码:119-124
英文摘要	A simultaneous determination method for caffeine, theobromine, and theophylline in chocolate was developed. Three compounds were ultrasonically extracted twice (15 min at 50t) in an acetonitrile water (1 : 1, v/v). The extract was purified using Oasis HLB SPE cartridge, and the purified processed by LC -MS. The method exhibited recoveries of 97.4-100.2%, RSDs of repeatability of 1.02.8%, and RSDs of within -laboratory reproducibility of 2.0-7.9%. This method was simpler and more selective than existing methods, and was practical for caffeine, theobromine, and theophylline analysis in chocolate.
英文关键词	caffeine theobromine theophylline chocolate
类型	Article
语种	日语
收录类别	SCI-E
WOS记录号	WOS:000697567000002
WOS关键词	COCOA
WOS类目	Food Science & Technology
WOS研究方向	Food Science & Technology
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/363249
作者单位	[Tanaka, Tomoya; Kimura, Keisuke; Kan, Kimiko; Shindo, Tetsuya; Sasamoto, Takeo] Tokyo Metropolitan Inst Publ Hlth, Shinjuku Ku, 3-24-1 Hyakunin Cho, Tokyo 1690073, Japan
推荐引用方式 GB/T 7714	Tanaka, Tomoya,Kimura, Keisuke,Kan, Kimiko,et al. Determination of Caffeine, Theobromine, and Theophylline in Chocolate Using LC-MS[J],2021,62(4):119-124.
APA	Tanaka, Tomoya,Kimura, Keisuke,Kan, Kimiko,Shindo, Tetsuya,&Sasamoto, Takeo.(2021).Determination of Caffeine, Theobromine, and Theophylline in Chocolate Using LC-MS.FOOD HYGIENE AND SAFETY SCIENCE,62(4),119-124.
MLA	Tanaka, Tomoya,et al."Determination of Caffeine, Theobromine, and Theophylline in Chocolate Using LC-MS".FOOD HYGIENE AND SAFETY SCIENCE 62.4(2021):119-124.