干旱区生态环境知识资源中心(Arid): An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters

Arid

	An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters
	Zhu Feng; Yao Zhijian; Ji Wenliang; Liu Deye; Zhang Hao; Li Aimin; Huo Zongli; Zhou Qing
来源期刊	Frontiers of Environmental Science & Engineering
ISSN	2095-2201
出版年	2020
卷号	14 期号:3
英文摘要	In this study,a hydrophilic resin named GCHM was fabricated based on poly(N-vinyl pyrrolidone-codivinylbenzene),characterized,and applied as a solid-phase extraction (SPE) material.Up to 44 pharmaceuticals and personal care products (PPCPs) belonging to 10 classes were recovered in environmental water samples.Different variables affecting extraction,such as adsorbent amount,sample pH,and loading speed,were optimized.Under optimal conditions,the average absolute recovery of 44 PPCPs was 75.6% using GCHM,indicating a better performance than the commercial Oasis HLB.SPE with home-made hydrophilic polymeric sorbent followed by ultra-performance liquid chromatography and tandem mass spectrometry was validated,and the method achieved good linearity (r~2 >0.991,for all analytes).In addition,the method detection limits of target compounds ranged from 0.03 to 0.6 ng/L.The developed method was applied to determine PPCPs in 10 environmental water samples taken from the Yangtze River,Huaihe River,and Taihu Lake,1 groundwater sample from Changzhou in Jiangsu Province,1 wastewater sample from Xiamen and 2 seawater samples from the Jiulong River in Fujian Province,China.In these samples,22 compounds were determined at levels ranging from 0.5 to 1590 ng/L.
英文关键词	Hydrophilic resin Solid phase extraction Pharmaceuticals and personal care product Ultra-performance liquid chromatography and tandem mass spectrometry Environmental water
类型	Article
语种	英语
收录类别	CSCD
WOS研究方向	Environmental Sciences & Ecology
CSCD记录号	CSCD:6791165
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/336334
作者单位	Zhu Feng, Jiangsu Provincial Center for Disease Control and Prevention, Nanjing, Jiangsu 210009, China.; Ji Wenliang, Jiangsu Provincial Center for Disease Control and Prevention, Nanjing, Jiangsu 210009, China.; Liu Deye, Jiangsu Provincial Center for Disease Control and Prevention, Nanjing, Jiangsu 210009, China.; Zhang Hao, Jiangsu Provincial Center for Disease Control and Prevention, Nanjing, Jiangsu 210009, China.; Huo Zongli, Jiangsu Provincial Center for Disease Control and Prevention, Nanjing, Jiangsu 210009, China.; Yao Zhijian, School of the Environment,Nanjing University;;Jiangsu Guochuang Enviro-protection Technology Co.Ltd., State Key Laboratory of Pollution Control and Resource Reuse;;, Nanjing;;Nanjing, ;; 210023;;211100.; Zhou Qing, School of the Environment,Nanjing University;;Jiangsu Guochuang Enviro-protection Technology Co.Ltd., State Key Laboratory of Pollution Control and Resource Reuse;;, Nanjing;;Nanjing, ;; 210023;;211100.; Li Aimin, School of the Environment,Nanjing University, S...
推荐引用方式 GB/T 7714	Zhu Feng,Yao Zhijian,Ji Wenliang,et al. An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters[J],2020,14(3).
APA	Zhu Feng.,Yao Zhijian.,Ji Wenliang.,Liu Deye.,Zhang Hao.,...&Zhou Qing.(2020).An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters.Frontiers of Environmental Science & Engineering,14(3).
MLA	Zhu Feng,et al."An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters".Frontiers of Environmental Science & Engineering 14.3(2020).