干旱区生态环境知识资源中心(Arid): Presence of benzotriazoles, benzothiazoles and benzenesulfonamides in surface water samples by liquid chromatography coupled to high-resolution mass spectrometry

Arid

DOI	10.1002/sscp.201800140
	Presence of benzotriazoles, benzothiazoles and benzenesulfonamides in surface water samples by liquid chromatography coupled to high-resolution mass spectrometry
	Hidalgo-Serrano, Miriam; Borrull, Francesc; Marce, Rosa M.; Pocurull, Eva
通讯作者	Marce, RM
来源期刊	SEPARATION SCIENCE PLUS
ISSN	2573-1815
出版年	2019
卷号	2 期号:3 页码:72-80
英文摘要	An analytical method has been developed for the simultaneous determination of seven benzotriazole, five benzothiazole and four benzenesulfonamide derivatives in surface water samples. The procedure is based on solid-phase extraction with Oasis HLB, followed by high-performance liquid chromatography coupled to high-resolution mass spectrometry. Apparent recoveries ranged from 40 to 101%, except for compounds the matrix effect of which was above -60%. The repeatability (n = 5) of the method was below 20% for all compounds except 4-hydroxybenzotriazole in river water. The method limits of detection for most compounds ranged from 1 to 12 ng/L for both river water and seawater. The method was then used for the determination of the studied compounds in several river water and seawater samples from harbour and coastal areas. 1-H-Benzotriazole (up to 78 ng/L in river water and above the upper limit of the calibration curve in seawater) and 4-methyl-1-H-benzotriazole (up to 44 ng/L in river water and 338 ng/L in seawater) were the most abundant compounds quantified in the samples, even though 5-methyl-1-H-benzotriazole and 2-hydroxybenzothiazole were also found in most samples. Some compounds were frequently found in certain types of samples, such as 2-aminobenzothiazole in river water. Benzenesulfonamide derivatives could not be quantified in any sample.
英文关键词	Benzenesulfonamides Benzothiazoles Benzotriazoles High-resolution mass spectrometry Surface water
类型	Article
语种	英语
收录类别	ESCI
WOS记录号	WOS:000476952900001
WOS关键词	SOLID-PHASE EXTRACTION ; DETERMINE POLAR BENZOTRIAZOLE ; AQUEOUS MATRICES ; WASTE-WATER ; CONTAMINANTS ; GAS ; TOXICITY ; DRUGS ; FATE
WOS类目	Chemistry, Analytical
WOS研究方向	Chemistry
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/333706
作者单位	[Hidalgo-Serrano, Miriam; Borrull, Francesc; Marce, Rosa M.; Pocurull, Eva] Univ Rovira & Virgili, Dept Analyt Chem & Organ Chem, Marcelli Domingo S-N, E-43007 Tarragona, Spain
推荐引用方式 GB/T 7714	Hidalgo-Serrano, Miriam,Borrull, Francesc,Marce, Rosa M.,et al. Presence of benzotriazoles, benzothiazoles and benzenesulfonamides in surface water samples by liquid chromatography coupled to high-resolution mass spectrometry[J],2019,2(3):72-80.
APA	Hidalgo-Serrano, Miriam,Borrull, Francesc,Marce, Rosa M.,&Pocurull, Eva.(2019).Presence of benzotriazoles, benzothiazoles and benzenesulfonamides in surface water samples by liquid chromatography coupled to high-resolution mass spectrometry.SEPARATION SCIENCE PLUS,2(3),72-80.
MLA	Hidalgo-Serrano, Miriam,et al."Presence of benzotriazoles, benzothiazoles and benzenesulfonamides in surface water samples by liquid chromatography coupled to high-resolution mass spectrometry".SEPARATION SCIENCE PLUS 2.3(2019):72-80.