干旱区生态环境知识资源中心(Arid): Simultaneous determination of 22 typical pharmaceuticals and personal care products in environmental water using ultra performance liquid chromatography-triple quadrupole mass spectrometry

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DOI	10.3724/SP.J.1123.2015.04019
	Simultaneous determination of 22 typical pharmaceuticals and personal care products in environmental water using ultra performance liquid chromatography-triple quadrupole mass spectrometry
	Wu Chunying; Gu Feng; Bai Lu; Lu Wenlong
通讯作者	Wu, CY
来源期刊	CHINESE JOURNAL OF CHROMATOGRAPHY
ISSN	1000-8713
出版年	2015
卷号	33 期号:8 页码:843-848
英文摘要	An analytical method for simultaneous determination of 22 typical pharmaceuticals and personal care products (PPCPs) in environmental water samples was developed by ultra performance liquid chromatography-triple quadrupole mass spectrometry (UPLC-MS/MS). An Oasis HLB solid phase extraction cartridge, methanol as washing solution, water containing 0. 1% formic acid-methanol (7 : 3, v/v) as the mobile phases were selected for sample pretreatment and chromatographic separation. Based on the optimized sample pretreatment procedures and separation condition, the target recoveries ranged from 73% to 125% in water with the relative standard deviations (RSDs) from 8.8% to 17.5%, and the linear ranges were from 2 to 2 000 mu g/L with correlation coefficients (R-2) not less than 0.997. The method can be applied to simultaneous determination of the 22 typical PPCPs in environmental water samples because of its low detection limits and high recoveries. It can provide support and help for the related research on water environmental risk assessment and control of the micro-organic pollutants.
英文关键词	solid phase extraction (SPE) ultra performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) pharmaceuticals personal care products (PPCPs) environmental water
类型	Article
语种	中文
收录类别	ESCI
WOS记录号	WOS:000435255600011
WOS类目	Chemistry, Analytical
WOS研究方向	Chemistry
来源机构	清华大学
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/331407
作者单位	[Wu Chunying; Gu Feng; Bai Lu; Lu Wenlong] Jilin Inst Chem Technol, Sch Resources & Environm Engn, Jilin 132022, Jilin, Peoples R China; [Wu Chunying] Tsinghua Univ, Sch Environm, State Key Lab Environm Simulat & Pollut Control, Beijing 100084, Peoples R China
推荐引用方式 GB/T 7714	Wu Chunying,Gu Feng,Bai Lu,et al. Simultaneous determination of 22 typical pharmaceuticals and personal care products in environmental water using ultra performance liquid chromatography-triple quadrupole mass spectrometry[J]. 清华大学,2015,33(8):843-848.
APA	Wu Chunying,Gu Feng,Bai Lu,&Lu Wenlong.(2015).Simultaneous determination of 22 typical pharmaceuticals and personal care products in environmental water using ultra performance liquid chromatography-triple quadrupole mass spectrometry.CHINESE JOURNAL OF CHROMATOGRAPHY,33(8),843-848.
MLA	Wu Chunying,et al."Simultaneous determination of 22 typical pharmaceuticals and personal care products in environmental water using ultra performance liquid chromatography-triple quadrupole mass spectrometry".CHINESE JOURNAL OF CHROMATOGRAPHY 33.8(2015):843-848.