干旱区生态环境知识资源中心(Arid): Determination of bisphenol diglycidyl ether residues in canned foodstuffs by high performance liquid chromatography-tandem mass spectrometry

Arid

DOI	10.3724/SP.J.1123.2012.08024
	Determination of bisphenol diglycidyl ether residues in canned foodstuffs by high performance liquid chromatography-tandem mass spectrometry
	Zhao Xiaoya; Fu Xiaofang; Wang Peng; Li Jing; Hu Xiaozhong
通讯作者	Zhao, XY
来源期刊	CHINESE JOURNAL OF CHROMATOGRAPHY
ISSN	1000-8713
出版年	2012
卷号	30 期号:10 页码:1002-1007
英文摘要	An accurate quantitative determination and confirmative method for bisphenol diglycidyl ether residues, bisphenol A diglycidyl ether (BADGE), bisphenol F diglycidyl ether (BFDGE), bisphenol A (2,3-dihydroxypropyl) glycidyl ether (BADGE center dot H2O), bisphenol A bis (2,3-dihydroxypropyl) ether (BADGE center dot 2H(2)O), bisphenol A (3-chloro-2-hydroxy propyl)(2,3dihy droxypropyl) ether (BADGE center dot H2O center dot HCl), bisphenol A (3-chloro-2-hydroxypropyl) glycidyl ether (BADGE center dot HCl), bisphenol A bis(3-chloro-2-hydroxypropyl) ether (BADGE center dot 2HCl), bisphenol F bis (2,3-dihydroxypropyl) ether (BFDGE center dot 2H(2)O), bisphenol F bis (3-chloro-2-hydroxypropyl) ether (BFDGE center dot 2HCl) in canned foodstuffs by high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) has been established. The sample was extracted with tert-butylmethyl ether and the extract was cleaned-up and concentrated on a Waters Oasis HLB column. The target compounds were analyzed by HPLC-MS/MS on a C-18 column by the gradient elution with methanol and 5 mmol/L ammonium acetate containing 0. 1% formic acid in a multiple reaction monitoring (MRM) scan mode. External matrix standard solutions were used for the quantitative determination and the calibration curves showed good linearity in the concentration range of 10. 0 - 2 000. 0 mu g/L for the nine target compounds. The limits of quantification of the nine compounds were 10. 0 mu g/kg (S/N >= 10). The average recoveries of the nine compounds ranged from 79. 6% to 100. 9% at the spiked levels of 10. 0, 100. 0, 1 000. 0 mu g/kg with the relative standard deviations (RSDs) of 6. 3% - 12. 1%. The method is sensitive, accurate, and suitable for the rapid determination of bisphenol diglycidyl ether residues in canned foodstuffs.
英文关键词	high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) bisphenol diglycidyl ethers canned foodstuffs
类型	Article
语种	中文
收录类别	ESCI
WOS记录号	WOS:000434511400005
WOS类目	Chemistry, Analytical
WOS研究方向	Chemistry
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/330170
作者单位	[Zhao Xiaoya; Fu Xiaofang; Wang Peng; Li Jing; Hu Xiaozhong] Hubei Entry Exit Inspect & Quarantine Bur, Wuhan 430050, Hubei, Peoples R China
推荐引用方式 GB/T 7714	Zhao Xiaoya,Fu Xiaofang,Wang Peng,et al. Determination of bisphenol diglycidyl ether residues in canned foodstuffs by high performance liquid chromatography-tandem mass spectrometry[J],2012,30(10):1002-1007.
APA	Zhao Xiaoya,Fu Xiaofang,Wang Peng,Li Jing,&Hu Xiaozhong.(2012).Determination of bisphenol diglycidyl ether residues in canned foodstuffs by high performance liquid chromatography-tandem mass spectrometry.CHINESE JOURNAL OF CHROMATOGRAPHY,30(10),1002-1007.
MLA	Zhao Xiaoya,et al."Determination of bisphenol diglycidyl ether residues in canned foodstuffs by high performance liquid chromatography-tandem mass spectrometry".CHINESE JOURNAL OF CHROMATOGRAPHY 30.10(2012):1002-1007.