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DOI10.1016/j.foodchem.2020.126450
Simultaneous extraction and separation of bioactive compounds from apple pomace using pressurized liquids coupled on-line with solid-phase extraction
da Silva, Laise C.; Souza, Mariana C.; Sumere, Beatriz R.; Silva, Luiz G. S.; da Cunha, Diogo T.; Barbero, Gerardo F.; Bezerra, Rosangela M. N.; Rostagno, Mauricio A.
通讯作者Rostagno, MA
来源期刊FOOD CHEMISTRY
ISSN0308-8146
EISSN1873-7072
出版年2020
卷号318
英文摘要The objective of this work was the development of an on-line extraction/fractionation method based on the coupling of pressurized liquid extraction and solid-phase extraction for the separation of phenolic compounds from apple pomace. Several variables of the process were evaluated, including the amount of water of the first stage (0-120 mL), temperature (60-80 degrees C), solid-phase extraction adsorbent (Sepra, Isolute, Strata X and Oasis) and activation/elution solvent (methanol and ethanol). The best results were observed with the adsorbent Sepra. The temperature had a small effect on recovery, but significant differences were observed for phlorizin and a quercetin derivative. Results indicate that ethanol can be used to replace methanol as an activation, extraction/elution solvent. While using mostly green solvents (water, ethanol, and a small amount of methanol that could be reused), the developed method produced higher or similar yields of acids (2.85 +/- 0.19 mg/g) and flavonoids (0.97 +/- 0.11 mg/g) than conventional methods.
英文关键词Apple pomace Phenolics Flavonoids Pressurized liquid extraction Solid-phase extraction
类型Article
语种英语
收录类别SCI-E
WOS记录号WOS:000520858000053
WOS关键词PHENOLIC-COMPOUNDS ; SAMPLE PREPARATION ; ISOFLAVONES ; FRUIT ; ULTRASOUND ; WATER ; ACIDS ; PEEL ; PULP
WOS类目Chemistry, Applied ; Food Science & Technology ; Nutrition & Dietetics
WOS研究方向Chemistry ; Food Science & Technology ; Nutrition & Dietetics
资源类型期刊论文
条目标识符http://119.78.100.177/qdio/handle/2XILL650/324312
作者单位[da Silva, Laise C.; Souza, Mariana C.; Sumere, Beatriz R.; Silva, Luiz G. S.; da Cunha, Diogo T.; Bezerra, Rosangela M. N.; Rostagno, Mauricio A.] Univ Estadual Campinas, Sch Appl Sci FCA, Multidisciplinary Lab Food & Hlth LabMAS, UNICAMP, Rua Pedro Zaccaria 1300, BR-13484350 Limeira, SP, Brazil; [Barbero, Gerardo F.] Univ Cadiz, Fac Sci, Dept Analyt Chem, IVAGRO,Agrifood Campus Int Excellence CeiA3, POB 40, Cadiz 11510, Spain
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GB/T 7714
da Silva, Laise C.,Souza, Mariana C.,Sumere, Beatriz R.,et al. Simultaneous extraction and separation of bioactive compounds from apple pomace using pressurized liquids coupled on-line with solid-phase extraction[J],2020,318.
APA da Silva, Laise C..,Souza, Mariana C..,Sumere, Beatriz R..,Silva, Luiz G. S..,da Cunha, Diogo T..,...&Rostagno, Mauricio A..(2020).Simultaneous extraction and separation of bioactive compounds from apple pomace using pressurized liquids coupled on-line with solid-phase extraction.FOOD CHEMISTRY,318.
MLA da Silva, Laise C.,et al."Simultaneous extraction and separation of bioactive compounds from apple pomace using pressurized liquids coupled on-line with solid-phase extraction".FOOD CHEMISTRY 318(2020).
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