干旱区生态环境知识资源中心(Arid): Determination of Moniliformin in Vegetable Oil by Solid-Phase Extraction-Hydrophilic Interaction Chromatography-Tandem Mass Spectrometry

Arid

DOI	10.1007/s10337-020-03901-3
	Determination of Moniliformin in Vegetable Oil by Solid-Phase Extraction-Hydrophilic Interaction Chromatography-Tandem Mass Spectrometry
	Chen, Rui 1,2; Li, Jiaxuan 3,4; Yang, Zhiwei 2; Zhang, Ang 2; Li, Xiang 2; Qi, Pengyu 2; Li, Jun 1; Zhang, Jinjie 2
通讯作者	Li, Jun ; Zhang, Jinjie
来源期刊	CHROMATOGRAPHIA
ISSN	0009-5893
EISSN	1612-1112
出版年	2020
卷号	83 期号:7 页码:903-907
英文摘要	An analytical method based on solid-phase extraction-hydrophilic interaction chromatography-tandem mass spectrometry (SPE-HILIC-MS/MS) has been developed to quantify moniliformin in vegetable oil. The sample was extracted by methanol and purified by an Oasis MAX solid-phase extraction column. Following purification, it was separated by a Waters HILIC hydrophilic interaction column. Acetonitrile and 0.5 mM ammonium acetate solution were used as a mobile phase for gradient elution. An electrospray-negative ion multiple-reaction monitoring mode was used to quantify moniliformin by external standard method. In the mass concentration range of 0.1-10 mu g/L, the correlation coefficient of moniliformin was 0.9997. The detection limit of this method was 0.03 mu g/L, and the limit of quantification was 0.1 mu g/L. When the three levels of 1.0, 2.0 and 5.0 mu g/kg moniliformin were added, the recovery was 84.6%-98.2% with a relative standard deviation of 1.3%-5.1%. The results indicated that this method is simple, fast, sensitive, reproducible, and can be used to determine moniliformin in vegetable oil.
英文关键词	HILIC-MS MS Solid-phase extraction Moniliformin Vegetable oil
类型	Article
语种	英语
国家	Peoples R China ; USA
收录类别	SCI-E
WOS记录号	WOS:000532657100002
WOS关键词	FUMONISINS B-1 ; MAIZE ; MYCOTOXINS ; PRODUCTS ; CORN
WOS类目	Biochemical Research Methods ; Chemistry, Analytical
WOS研究方向	Biochemistry & Molecular Biology ; Chemistry
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/319093
作者单位	1.Hebei Normal Univ Sci & Technol, Coll Food Sci & Technol, Qinhuangdao 066600, Hebei, Peoples R China; 2.Qinhuangdao Customs Tech Ctr, Qinhuangdao 066000, Hebei, Peoples R China; 3.Hebei Agr Univ, Coll Food Sci & Technol, Baoding 071000, Hebei, Peoples R China; 4.Univ Illinois, Dept Food Sci & Human Nutr, Urbana, IL 61801 USA
推荐引用方式 GB/T 7714	Chen, Rui,Li, Jiaxuan,Yang, Zhiwei,et al. Determination of Moniliformin in Vegetable Oil by Solid-Phase Extraction-Hydrophilic Interaction Chromatography-Tandem Mass Spectrometry[J],2020,83(7):903-907.
APA	Chen, Rui.,Li, Jiaxuan.,Yang, Zhiwei.,Zhang, Ang.,Li, Xiang.,...&Zhang, Jinjie.(2020).Determination of Moniliformin in Vegetable Oil by Solid-Phase Extraction-Hydrophilic Interaction Chromatography-Tandem Mass Spectrometry.CHROMATOGRAPHIA,83(7),903-907.
MLA	Chen, Rui,et al."Determination of Moniliformin in Vegetable Oil by Solid-Phase Extraction-Hydrophilic Interaction Chromatography-Tandem Mass Spectrometry".CHROMATOGRAPHIA 83.7(2020):903-907.