干旱区生态环境知识资源中心(Arid): Effect of Calcination Temperature of Musa sapientum Linn Peels as a Novel Biobased Heterogeneous Catalyst for Soybean Oil-derived Fatty Acid Methyl Ester Formation

Arid

	Effect of Calcination Temperature of Musa sapientum Linn Peels as a Novel Biobased Heterogeneous Catalyst for Soybean Oil-derived Fatty Acid Methyl Ester Formation
	Jitjamnong, Jakkrapong 1; Thunyaratchatanon, Chachchaya 2; Luengnaruemitchai, Apanee 2,3; Kongrit, Napaphat 1; Kasetsomboon, Naparat 1; Chuaykarn, Narinphop 4; Khantikulanon, Nonlapan 5
通讯作者	Jitjamnong, Jakkrapong
来源期刊	CHIANG MAI JOURNAL OF SCIENCE
ISSN	0125-2526
出版年	2020
卷号	47 期号:3 页码:484-498
英文摘要	In the present study, a novel solid base catalyst derived from desert banana (Musa sapientum Linn) peels was used as a catalyst for biodiesel production. The catalyst was calcined at several temperatures between 550-650 degrees C under atmosphere pressure for 4 h. The composition, structure and texture of the calcined banana peel (CBP) catalysts were characterized by X-ray diffraction, thermogravimetric analysis, scanning electron microscopy with energy dispersive spectroscopy, X-ray fluorescence spectrophotometry, and Fourier-transform infrared spectroscopy analyses. The fatty acid profile of the feed soybean oil and the fatty acid methyl ester (FAME) product composition was analyzed using gas chromatography with flame ionization detection. The prepared catalysts were then applied for the catalytic transesterification of soybean oil with methanol under microwave-assisted heating to form FAME. The effect of the calcination temperature in the catalyst preparation, the catalyst loading level, reaction time, methanol: soybean oil molar ratio and catalyst reusability on the FAME yield were determined by univariate analysis. The CBP catalyst synthesized at 600 degrees C exhibited the highest catalytic activity, since the calcined ash was rich in K, P, Ca and Mg which formed a basic heterogenous catalyst at this calcination temperature. At the determined optimal reaction condition (1 wt.% catalyst loading level, 12:1 molar ratio of methanol: soybean oil, and a 2 min of reaction time under 300 W microwave irradiation) a FAME yield of 99.3% was obtained. Furthermore, the catalyst showed a good reusability with a biodiesel yield of more than 80.7% after four uses.
英文关键词	Musa sapientum Linn peels biodiesel transesterification heterogeneous catalyst catalyst reusability
类型	Article
语种	英语
国家	Thailand
收录类别	SCI-E
WOS记录号	WOS:000528210800010
WOS关键词	IRRADIATION-ASSISTED TRANSESTERIFICATION ; BIODIESEL PRODUCTION ; SEED OIL ; PALM OIL ; POD HUSK ; WASTE ; OPTIMIZATION ; BIOMASS ; CONVERSION
WOS类目	Multidisciplinary Sciences
WOS研究方向	Science & Technology - Other Topics
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/318604
作者单位	1.Rajamangala Univ Technol Srivijaya, Fac Ind Educ & Technol, Dept Petr Technol, Songkhla 90000, Thailand; 2.Chulalongkorn Univ, Petr & Petrochem Coll, Bangkok 10330, Thailand; 3.Chulalongkorn Univ, Ctr Excellence Catalysis Bioenergy & Renewable Ch, Bangkok 10330, Thailand; 4.Rajamangala Univ Technol Srivijaya, Fac Liberal Arts, Dept Food & Nutr, Songkhla 90000, Thailand; 5.Valaya Alongkorn Rajabhat Univ, Fac Publ Hlth, Dept Environm Hlth, Pathum Thani 10120, Thailand
推荐引用方式 GB/T 7714	Jitjamnong, Jakkrapong,Thunyaratchatanon, Chachchaya,Luengnaruemitchai, Apanee,et al. Effect of Calcination Temperature of Musa sapientum Linn Peels as a Novel Biobased Heterogeneous Catalyst for Soybean Oil-derived Fatty Acid Methyl Ester Formation[J],2020,47(3):484-498.
APA	Jitjamnong, Jakkrapong.,Thunyaratchatanon, Chachchaya.,Luengnaruemitchai, Apanee.,Kongrit, Napaphat.,Kasetsomboon, Naparat.,...&Khantikulanon, Nonlapan.(2020).Effect of Calcination Temperature of Musa sapientum Linn Peels as a Novel Biobased Heterogeneous Catalyst for Soybean Oil-derived Fatty Acid Methyl Ester Formation.CHIANG MAI JOURNAL OF SCIENCE,47(3),484-498.
MLA	Jitjamnong, Jakkrapong,et al."Effect of Calcination Temperature of Musa sapientum Linn Peels as a Novel Biobased Heterogeneous Catalyst for Soybean Oil-derived Fatty Acid Methyl Ester Formation".CHIANG MAI JOURNAL OF SCIENCE 47.3(2020):484-498.