干旱区生态环境知识资源中心(Arid): Simultaneous Determination of Malachite Green, Chloramphenicols, Sulfonamides, and Fluoroquinolones Residues in Fish by Liquid Chromatography-Mass Spectrometry

Arid

DOI	10.1155/2020/3725618
	Simultaneous Determination of Malachite Green, Chloramphenicols, Sulfonamides, and Fluoroquinolones Residues in Fish by Liquid Chromatography-Mass Spectrometry
	Chen, Yongping 1; Xia, Sudong 2; Han, Xianqin 1; Fu, Zhiru 1
通讯作者	Fu, Zhiru
来源期刊	JOURNAL OF ANALYTICAL METHODS IN CHEMISTRY
ISSN	2090-8865
EISSN	2090-8873
出版年	2020
卷号	2020
英文摘要	A fast-analytical method using simplified extraction has been developed for the simultaneous determination of 42 compounds from 4 different classes of veterinary drugs (amphenicols, triphenylmethane, fluoroquinolones, and sulfonamides) in fish by reverse phase liquid chromatography-tandem mass spectrometry. The selection of extraction reagents was optimized using different types of microfiltration membrane, mobile phase, and LC column. Samples were extracted using 0.4% hydrochloric acid in acetonitrile and ethyl acetate and then were cleaned up using solid-phase extraction Cleanert Alumina N columns (500 mg) and Oasis hydrophilic-lipophilic balance (HLB) cartridges. The chromatographic separation was performed on a XR-ODS C-8 column using a mobile phase of (A) 0.1% formic acid and 2 mM ammonium acetate and (B) 0.1% formic acid acetonitrile at a flow rate of 0.25 mL center dot min(-1). The results indicated 67.7-112.8% recovery of 42 compounds with an intra- and interday relative standard deviations less than 10%. The limits of quantification for analytes were in the range of 0.3-1.0 mu g kg(-1) for samples which were satisfactory to support future surveillance monitoring. The method applicability was checked by analyzing 30 fish samples collected from local markets. Two fish samples surpassed the established MRL of 100 mu g kg(-1) with values of 104 mu g kg(-1) and 112 mu g kg(-1).
类型	Article
语种	英语
国家	Peoples R China
开放获取类型	Green Published, gold
收录类别	SCI-E
WOS记录号	WOS:000518602500001
WOS关键词	SOLID-PHASE EXTRACTION ; QUINOLONE RESIDUES ; LEUCOMALACHITE GREEN ; CRYSTAL VIOLET ; HOT-WATER ; RAW-MILK ; ANTIBIOTICS ; BOVINE ; PRECONCENTRATION ; TETRACYCLINES
WOS类目	Chemistry, Analytical
WOS研究方向	Chemistry
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/314854
作者单位	1.Tianjin Agr Ecol Environm Monitoring & Agr Prod Q, Tianjin 300221, Peoples R China; 2.Tianjin Agr Univ, Dept Fishery Sci, Tianjin Key Lab Aqua Ecol & Aquaculture, Tianjin 300384, Peoples R China
推荐引用方式 GB/T 7714	Chen, Yongping,Xia, Sudong,Han, Xianqin,et al. Simultaneous Determination of Malachite Green, Chloramphenicols, Sulfonamides, and Fluoroquinolones Residues in Fish by Liquid Chromatography-Mass Spectrometry[J],2020,2020.
APA	Chen, Yongping,Xia, Sudong,Han, Xianqin,&Fu, Zhiru.(2020).Simultaneous Determination of Malachite Green, Chloramphenicols, Sulfonamides, and Fluoroquinolones Residues in Fish by Liquid Chromatography-Mass Spectrometry.JOURNAL OF ANALYTICAL METHODS IN CHEMISTRY,2020.
MLA	Chen, Yongping,et al."Simultaneous Determination of Malachite Green, Chloramphenicols, Sulfonamides, and Fluoroquinolones Residues in Fish by Liquid Chromatography-Mass Spectrometry".JOURNAL OF ANALYTICAL METHODS IN CHEMISTRY 2020(2020).