干旱区生态环境知识资源中心(Arid): An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters

Arid

DOI	10.1007/s11783-020-1228-y
	An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters
	Zhu, Feng 1; Yao, Zhijian 2,3; Ji, Wenliang 1; Liu, Deye 1; Zhang, Hao 1; Li, Aimin 2; Huo, Zongli 1; Zhou, Qing 2,3
通讯作者	Huo, Zongli ; Zhou, Qing
来源期刊	FRONTIERS OF ENVIRONMENTAL SCIENCE & ENGINEERING
ISSN	2095-2201
EISSN	2095-221X
出版年	2020
卷号	14 期号:3
英文摘要	In this study, a hydrophilic resin named GCHM was fabricated based on poly(N-vinyl pyrrolidone-co-divinylbenzene), characterized, and applied as a solid-phase extraction (SPE) material. Up to 44 pharmaceuticals and personal care products (PPCPs) belonging to 10 classes were recovered in environmental water samples. Different variables affecting extraction, such as adsorbent amount, sample pH, and loading speed, were optimized. Under optimal conditions, the average absolute recovery of 44 PPCPs was 75.6% using GCHM, indicating a better performance than the commercial Oasis(R) HLB. SPE with home-made hydrophilic polymeric sorbent followed by ultra-performance liquid chromatography and tandem mass spectrometry was validated, and the method achieved good linearity (r(2) >0.991, for all analytes). In addition, the method detection limits of target compounds ranged from 0.03 to 0.6 ng/L. The developed method was applied to determine PPCPs in 10 environmental water samples taken from the Yangtze River, Huaihe River, and Taihu Lake, 1 groundwater sample from Changzhou in Jiangsu Province, 1 wastewater sample from Xiamen and 2 seawater samples from the Jiulong River in Fujian Province, China. In these samples, 22 compounds were determined at levels ranging from 0.5 to 1590 ng/L.
英文关键词	Hydrophilic resin Solid phase extraction Pharmaceuticals and personal care product Ultra-performance liquid chromatography and tandem mass spectrometry Environmental water
类型	Article
语种	英语
国家	Peoples R China
收录类别	SCI-E
WOS记录号	WOS:000519690400001
WOS关键词	ENDOCRINE DISRUPTING CHEMICALS ; MASS-SPECTROMETRY ANALYSIS ; N-VINYL PYRROLIDONE ; LIQUID-CHROMATOGRAPHY ; TREATMENT PLANTS ; DRINKING-WATER ; WASTE-WATER ; SURFACE ; PPCPS ; FATE
WOS类目	Engineering, Environmental ; Environmental Sciences
WOS研究方向	Engineering ; Environmental Sciences & Ecology
来源机构	南京大学
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/314567
作者单位	1.Jiangsu Prov Ctr Dis Control & Prevent, Nanjing 210009, Peoples R China; 2.Nanjing Univ, State Key Lab Pollut Control & Resource Reuse, Sch Environm, Nanjing 210023, Peoples R China; 3.Jiangsu Guochuang Enviroprotect Technol Co Ltd, 19 Changqing Ave, Nanjing 211100, Peoples R China
推荐引用方式 GB/T 7714	Zhu, Feng,Yao, Zhijian,Ji, Wenliang,et al. An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters[J]. 南京大学,2020,14(3).
APA	Zhu, Feng.,Yao, Zhijian.,Ji, Wenliang.,Liu, Deye.,Zhang, Hao.,...&Zhou, Qing.(2020).An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters.FRONTIERS OF ENVIRONMENTAL SCIENCE & ENGINEERING,14(3).
MLA	Zhu, Feng,et al."An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters".FRONTIERS OF ENVIRONMENTAL SCIENCE & ENGINEERING 14.3(2020).