干旱区生态环境知识资源中心(Arid): Determination of Ellagic Acid in Wine by Solid-Phase Extraction-Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry

Arid

DOI	10.1007/s12161-019-01438-2
	Determination of Ellagic Acid in Wine by Solid-Phase Extraction-Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry
	Chen, Rui 1,2; Li, Jiaxuan 3; Yang, Zhiwei 2; Gao, Fei 2; Qi, Pengyu 2; Li, Xiang 2; Zhu, Fengmei 1; Li, Jun 1; Zhang, Jinjie 2
通讯作者	Chen, Rui ; Li, Jun
来源期刊	FOOD ANALYTICAL METHODS
ISSN	1936-9751
EISSN	1936-976X
出版年	2019
卷号	12 期号:5 页码:1103-1110
英文摘要	The method for the determination of ellagic acid in wine by solid-phase extraction-ultra-high performance liquid chromatography-tandem mass spectrometry (SPE-UPLC-MS/MS) using electrospray ion source (ESI) multiple reaction monitoring (MRM) mode detection was established. The sample was purified by Oasis HLB solid-phase extraction column and separated on an Acquity UPLC (R) BEH C18 column (2.1mmx100mm 1.7m) with a mobile phase of 0.1% formic acid methanol-0.1% formic acid aqueous solution. Under the best detection conditions, ellagic acid within the range of 0.011mg/L had a good linear relationship with a correlation coefficient of 0.9993. The detection limit (LOD) and quantitative limit (LOQ) were 3 and 10g/L, respectively. The recovery was 90.8116% with the relative standard deviation (RSD) of 3.69.4%. The results indicate that the method is simple, fast, sensitive, and reproducible and can be used for the determination of ellagic acid in wine.
英文关键词	Solid-phase extraction UPLC-MS MS Ellagic acid Wine
类型	Article
语种	英语
国家	Peoples R China
收录类别	SCI-E
WOS记录号	WOS:000465965500007
WOS类目	Food Science & Technology
WOS研究方向	Food Science & Technology
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/215655
作者单位	1.Hebei Normal Univ Sci & Technol, Coll Food Sci & Technol, Qinhuangdao 066600, Hebei, Peoples R China; 2.Qinhuangdao Customs, Qinhuangdao 066000, Hebei, Peoples R China; 3.Hebei Agr Univ, Coll Food Sci & Technol, Baoding 071000, Hebei, Peoples R China
推荐引用方式 GB/T 7714	Chen, Rui,Li, Jiaxuan,Yang, Zhiwei,et al. Determination of Ellagic Acid in Wine by Solid-Phase Extraction-Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry[J],2019,12(5):1103-1110.
APA	Chen, Rui.,Li, Jiaxuan.,Yang, Zhiwei.,Gao, Fei.,Qi, Pengyu.,...&Zhang, Jinjie.(2019).Determination of Ellagic Acid in Wine by Solid-Phase Extraction-Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry.FOOD ANALYTICAL METHODS,12(5),1103-1110.
MLA	Chen, Rui,et al."Determination of Ellagic Acid in Wine by Solid-Phase Extraction-Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry".FOOD ANALYTICAL METHODS 12.5(2019):1103-1110.