干旱区生态环境知识资源中心(Arid): 高效液相色谱法同时测定禽肉中土霉素、四环素、金霉素、强力霉素残留的研究

Arid

	高效液相色谱法同时测定禽肉中土霉素、四环素、金霉素、强力霉素残留的研究
其他题名	Simultaneous Determination of Oxytetracycline, Tetracycline, Chlortetracycline and Doxycycline in Poultry Meat by High Performance Liquid Chromatography
	庞国芳; 曹彦忠; 张进杰; 贾光群; 范春林; 李学民
来源期刊	分析测试学报
ISSN	1004-4957
出版年	2005
卷号	24 期号:4 页码:61-63,66
中文摘要	建立了一种高效液相色谱法同时测定禽肉中土霉素、四环素、金霉素、强力霉素残留的分析方法.禽肉样品用0.1mol/L Na2EDTA-Mcllvaine缓冲溶液提取,清液用Oasis HLB固相萃取柱和Carboxvlic acid阴离子交换柱净化,用流动相洗脱定容后,用紫外检测器于350nm测定.在5～100mug/kg添加水平,回收率为60%～100%,相对标准偏差在16%以内.土霉素、四环素的检出限为2mug/kg,金霉素、强力霉素的检出限为5mug/kg.
英文摘要	A high perfonnance liquid chromatography method was developed for simultaneous determination of oxytetracycline, tetracycline, chlortetracycline and doxycycline residues in poultry meat. Samples were ex-tracted with 0. 1 mol/L NaiEDTA - Mcllvaine buffer solutions and centrifuged. The sample extracts were cleaned up by both Oasis HLB sol id-phase extraction cartridge and carbolic acid anion exchange cartridge and then were determined by UV detection at 350 nm. At fortification levels of 5 - 100 /Jg/kg, recoveries were 60% - 100% with coefficients of variation within 16% . Limit of detection was 2 Mg/kg for oxytetracycline and tetracycline and 5 ugAg for chlortetracycline and doxycycline.
中文关键词	禽肉 ; 土霉素 ; 四环素 ; 金霉素 ; 强力霉素 ; 固相萃取 ; 高效液相色谱
英文关键词	Poultry meat Oxytetracycline Tetracycline Chlortetracycline Doxycycline Solid-phase extrac-tion High performance liquid chromatography
语种	中文
国家	中国
收录类别	CSCD
WOS类目	CHEMISTRY ANALYTICAL
WOS研究方向	Chemistry
CSCD记录号	CSCD:1998540
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/206072
作者单位	秦皇岛出入境检验检疫局, 秦皇岛, 河北 066002, 中国
推荐引用方式 GB/T 7714	庞国芳,曹彦忠,张进杰,等. 高效液相色谱法同时测定禽肉中土霉素、四环素、金霉素、强力霉素残留的研究[J],2005,24(4):61-63,66.
APA	庞国芳,曹彦忠,张进杰,贾光群,范春林,&李学民.(2005).高效液相色谱法同时测定禽肉中土霉素、四环素、金霉素、强力霉素残留的研究.分析测试学报,24(4),61-63,66.
MLA	庞国芳,et al."高效液相色谱法同时测定禽肉中土霉素、四环素、金霉素、强力霉素残留的研究".分析测试学报 24.4(2005):61-63,66.