Arid
DOI10.1080/19440049.2015.1018341
Simultaneous determination of sweeteners in beverages by LC-MS/MS
Sakai, Hiroaki; Yamashita, Azusa; Tamura, Masayoshi; Uyama, Atsuo; Mochizuki, Naoki
通讯作者Mochizuki, Naoki
来源期刊FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT
ISSN1944-0049
EISSN1944-0057
出版年2015
卷号32期号:6页码:808-816
英文摘要

A new method was established for the simultaneous determination of 10 sweeteners and a degradation product in beverages by using LC-MS/MS. An ACQUITY UPLC BEH C18 (2.1x100mm, 1.7 mu m) was used as the LC column and 0.1% each of aqueous formic acid and formic acid in acetonitrile were used as the mobile phase. A simple and rapid determination of sweeteners was possible by diluting with a solvent, and in the case of some samples containing a large amount of foreign matter, after pre-treatment by diluting with solvent and clean-up of the sample using an Oasis HLB cartridge. All the validation results were satisfactory. As the regulations and standards for sweeteners vary from country to country, a field survey of 58 beverages marketed in Japan was performed using the present method. No issues concerning the labelling or food sanitation law were found in the tested samples.


英文关键词LC-MS/MS sweetener diketopiperazines sucralose aspartame beverage acesulfame potassium rebaudioside A
类型Article
语种英语
国家Japan
收录类别SCI-E
WOS记录号WOS:000354112400002
WOS关键词FOODS ; ASPARTAME
WOS类目Chemistry, Applied ; Food Science & Technology ; Toxicology
WOS研究方向Chemistry ; Food Science & Technology ; Toxicology
资源类型期刊论文
条目标识符http://119.78.100.177/qdio/handle/2XILL650/187297
作者单位Asahi Grp Holdings Ltd, Res Labs Food Safety Chem, Moriya, Ibaraki, Japan
推荐引用方式
GB/T 7714
Sakai, Hiroaki,Yamashita, Azusa,Tamura, Masayoshi,et al. Simultaneous determination of sweeteners in beverages by LC-MS/MS[J],2015,32(6):808-816.
APA Sakai, Hiroaki,Yamashita, Azusa,Tamura, Masayoshi,Uyama, Atsuo,&Mochizuki, Naoki.(2015).Simultaneous determination of sweeteners in beverages by LC-MS/MS.FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT,32(6),808-816.
MLA Sakai, Hiroaki,et al."Simultaneous determination of sweeteners in beverages by LC-MS/MS".FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT 32.6(2015):808-816.
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