Knowledge Resource Center for Ecological Environment in Arid Area
DOI | 10.1080/19440049.2015.1018341 |
Simultaneous determination of sweeteners in beverages by LC-MS/MS | |
Sakai, Hiroaki; Yamashita, Azusa; Tamura, Masayoshi; Uyama, Atsuo; Mochizuki, Naoki | |
通讯作者 | Mochizuki, Naoki |
来源期刊 | FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT
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ISSN | 1944-0049 |
EISSN | 1944-0057 |
出版年 | 2015 |
卷号 | 32期号:6页码:808-816 |
英文摘要 | A new method was established for the simultaneous determination of 10 sweeteners and a degradation product in beverages by using LC-MS/MS. An ACQUITY UPLC BEH C18 (2.1x100mm, 1.7 mu m) was used as the LC column and 0.1% each of aqueous formic acid and formic acid in acetonitrile were used as the mobile phase. A simple and rapid determination of sweeteners was possible by diluting with a solvent, and in the case of some samples containing a large amount of foreign matter, after pre-treatment by diluting with solvent and clean-up of the sample using an Oasis HLB cartridge. All the validation results were satisfactory. As the regulations and standards for sweeteners vary from country to country, a field survey of 58 beverages marketed in Japan was performed using the present method. No issues concerning the labelling or food sanitation law were found in the tested samples. |
英文关键词 | LC-MS/MS sweetener diketopiperazines sucralose aspartame beverage acesulfame potassium rebaudioside A |
类型 | Article |
语种 | 英语 |
国家 | Japan |
收录类别 | SCI-E |
WOS记录号 | WOS:000354112400002 |
WOS关键词 | FOODS ; ASPARTAME |
WOS类目 | Chemistry, Applied ; Food Science & Technology ; Toxicology |
WOS研究方向 | Chemistry ; Food Science & Technology ; Toxicology |
资源类型 | 期刊论文 |
条目标识符 | http://119.78.100.177/qdio/handle/2XILL650/187297 |
作者单位 | Asahi Grp Holdings Ltd, Res Labs Food Safety Chem, Moriya, Ibaraki, Japan |
推荐引用方式 GB/T 7714 | Sakai, Hiroaki,Yamashita, Azusa,Tamura, Masayoshi,et al. Simultaneous determination of sweeteners in beverages by LC-MS/MS[J],2015,32(6):808-816. |
APA | Sakai, Hiroaki,Yamashita, Azusa,Tamura, Masayoshi,Uyama, Atsuo,&Mochizuki, Naoki.(2015).Simultaneous determination of sweeteners in beverages by LC-MS/MS.FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT,32(6),808-816. |
MLA | Sakai, Hiroaki,et al."Simultaneous determination of sweeteners in beverages by LC-MS/MS".FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT 32.6(2015):808-816. |
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