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DOI10.1080/17518253.2014.944940
A simple method for simultaneous determination of nine triazines in drinking water
Beceiro-Gonzalez, Elisa; Gonzalez-Castro, Maria J.; Pouso-Blanco, Rebeca; Muniategui-Lorenzo, Soledad; Lopez-Mahia, Purificacion; Prada-Rodriguez, Dario
通讯作者Beceiro-Gonzalez, Elisa
来源期刊GREEN CHEMISTRY LETTERS AND REVIEWS
ISSN1751-8253
EISSN1751-7192
出版年2014
卷号7期号:3页码:271-277
英文摘要

A simple, effective, and economic method for determination of nine triazines (ametryn, atrazine, cyanazine, prometryn, propazine, simazine, simetryn, terbuthylazine, and terbutryn) in drinking water based on solid-phase extraction (SPE) followed by high-performance liquid chromatography-diode array detection (HPLC-DAD) was developed. A specialized solid phase (Oasis HLB) was used, and the parameters that may affect the efficiency of SPE were optimized. The limits of detection (ranged from 0.010 to 0.023 mu g L-1) were satisfactory and allow the determination of triazines at the levels required by European Union legislation. Repeatability (2.4-7.6%) and intermediate precision (0.9-11.0%) calculated at 0.1 mu g L-1 (legislation level) were adequate. The accuracy calculated as the average recovery of spiked tap and mineral waters was higher than 86% for all compounds. The developed method also could be used for undergraduate laboratory experiments because it acquaints students with solution preparation, solid phase extraction procedure, and HPLC-DAD technique.


英文关键词water analysis triazines SPE HPLC-DAD
类型Article
语种英语
国家Spain
收录类别SCI-E
WOS记录号WOS:000341004800009
WOS关键词PERFORMANCE LIQUID-CHROMATOGRAPHY ; SOLID-PHASE EXTRACTION ; TANDEM MASS-SPECTROMETRY ; MOLECULARLY IMPRINTED POLYMERS ; BAR SORPTIVE EXTRACTION ; CARBON NANOTUBES ; SURFACE WATERS ; RIVER WATER ; HERBICIDES ; SAMPLES
WOS类目Chemistry, Multidisciplinary ; Green & Sustainable Science & Technology
WOS研究方向Chemistry ; Science & Technology - Other Topics
资源类型期刊论文
条目标识符http://119.78.100.177/qdio/handle/2XILL650/182369
作者单位Univ A Coruna, Fac Sci, Dept Analyt Chem, Grp QANAP, La Coruna, Spain
推荐引用方式
GB/T 7714
Beceiro-Gonzalez, Elisa,Gonzalez-Castro, Maria J.,Pouso-Blanco, Rebeca,et al. A simple method for simultaneous determination of nine triazines in drinking water[J],2014,7(3):271-277.
APA Beceiro-Gonzalez, Elisa,Gonzalez-Castro, Maria J.,Pouso-Blanco, Rebeca,Muniategui-Lorenzo, Soledad,Lopez-Mahia, Purificacion,&Prada-Rodriguez, Dario.(2014).A simple method for simultaneous determination of nine triazines in drinking water.GREEN CHEMISTRY LETTERS AND REVIEWS,7(3),271-277.
MLA Beceiro-Gonzalez, Elisa,et al."A simple method for simultaneous determination of nine triazines in drinking water".GREEN CHEMISTRY LETTERS AND REVIEWS 7.3(2014):271-277.
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