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Groundwater contamination is one of the most significant problems in arid countries. Al-Quwiy’yia region is an example of an area where the groundwater is contaminated as a result of infiltration of waste water in low-lying areas adjacent to inhabited zones. Such contamination poses significant environmental threats for the surrounding environment and groundwater. Surface observations and spatial distribution of contamination observed in the shallow aquifer indicate that the main contamination sources were from sewage as well as from waste water dumping. However, the main source of water supply for the whole area is groundwater abstracted from the relatively shallow aquifer. Therefore, the transient electromagnetic method (TEM) and 2D electrical resistivity tomography (2D ERT) have been applied close to the waste water dump site to characterize the response of pollution plumes. Both of these geoelectrical techniques are sensitive to electrical conductivity as well as to other physical properties, which are greatly influenced by the polluted groundwater. Therefore, it is possible to profile the contamination plumes, both vertically and horizontally, in the vicinity of the measured stations. The ERT profiles gave detailed information about the lateral distribution of the contaminated groundwater, whereas the TEM demonstrated the vertical extensions.