干旱区生态环境知识资源中心(Arid): Detection of Benzo[a]pyrene in Fried Food by Ultrasound-Assisted Matrix Solid-Phase Dispersion and Isotope Dilution GC-MS

Arid

DOI	10.1007/s10337-013-2575-7
	Detection of Benzo[a]pyrene in Fried Food by Ultrasound-Assisted Matrix Solid-Phase Dispersion and Isotope Dilution GC-MS
	Liu, Hongcheng; Shao, Jinliang; Lin, Tao; Li, Qiwan
通讯作者	Li, Qiwan
来源期刊	CHROMATOGRAPHIA
ISSN	0009-5893
EISSN	1612-1112
出版年	2013
卷号	76 期号:23-24 页码:1785-1789
英文摘要	A simple, sensitive and reliable analytical method was developed for the detection of benzo[a]pyrene in fried food using gas chromatography-mass spectrometry with an isotope-labelled internal standard. Samples were directly extracted and purified by the ultrasound-assisted matrix solid-phase dispersion (MSPD) procedure. The simple pretreatment procedures were tested with different absorbents (C18, NH2, Oasis, and SiO2). The optimal ultrasonication-assisted MSPD was achieved by MSPD-SiO2 and sonication for 10 min in an ultrasonic bath. The samples were quantified using benzo[a]pyrene-d(12) as the internal standard. An analysis of the samples spiked with different levels of benzo[a]pyrene showed recoveries ranging from 84.6 to 103.2 %, with an RSD of 3.21-8.32 %, depending on the spiking level. This method was thus shown to be suitable for the detection of benzo[a]pyrene in fried food.
英文关键词	GC-MS Ultrasound-assisted matrix solid-phase dispersion Benzo[a]pyrene Fried food
类型	Article
语种	英语
国家	Peoples R China
收录类别	SCI-E
WOS记录号	WOS:000327433500026
WOS关键词	POLYCYCLIC AROMATIC-HYDROCARBONS ; PERFORMANCE LIQUID-CHROMATOGRAPHY ; VEGETABLE-OILS ; EDIBLE OILS ; EXTRACTION ; SAMPLES
WOS类目	Biochemical Research Methods ; Chemistry, Analytical
WOS研究方向	Biochemistry & Molecular Biology ; Chemistry
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/176421
作者单位	Yunnan Acad Agr Sci, Inst Qual Standard & Testing Technol, Minist Agr, Lab Qual & Safety Risk Assessment Agroprod Kunmin, Kunming 650223, Peoples R China
推荐引用方式 GB/T 7714	Liu, Hongcheng,Shao, Jinliang,Lin, Tao,et al. Detection of Benzo[a]pyrene in Fried Food by Ultrasound-Assisted Matrix Solid-Phase Dispersion and Isotope Dilution GC-MS[J],2013,76(23-24):1785-1789.
APA	Liu, Hongcheng,Shao, Jinliang,Lin, Tao,&Li, Qiwan.(2013).Detection of Benzo[a]pyrene in Fried Food by Ultrasound-Assisted Matrix Solid-Phase Dispersion and Isotope Dilution GC-MS.CHROMATOGRAPHIA,76(23-24),1785-1789.
MLA	Liu, Hongcheng,et al."Detection of Benzo[a]pyrene in Fried Food by Ultrasound-Assisted Matrix Solid-Phase Dispersion and Isotope Dilution GC-MS".CHROMATOGRAPHIA 76.23-24(2013):1785-1789.