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DOI10.1365/s10337-010-1575-0
Low-Level Determination of Organochlorine Pesticides in Wines by Automatic Preconcentration and GC-MS-MS Detection
Antonio Perez-Serradilla, Jose1; Maria Mata-Granados, Jose1,2; Luque de Castro, Maria Dolores1
通讯作者Luque de Castro, Maria Dolores
来源期刊CHROMATOGRAPHIA
ISSN0009-5893
出版年2010
卷号71期号:9-10页码:899-905
英文摘要

Solid-phase extraction using automated equipment has been applied to different types of wine (red, white, sparkling and ros,) spiked with 16 organochlorine pesticides (OCPs) for their preconcentration. PRPS, Oasis HLB, Hysphere Resin SH, Resin GP, C8 and C18 sorbent cartridges were tested. The separation-detection step was carried out by gas chromatography-tandem mass spectrometry. Changes in both the volume flushed through the sorbent (ranging between 25 and 100 mL) and the volume injected into the chromatograph (1 or 10 mu L) allow the detection limits of the method to be adapted to the analytes contents in the target samples. Preconcentrating 100 mL of wine and injecting into the chromatrograph 10 mu L of extract, limits of detection obtained for the OPCs range between 1.7 and 9.7 ng L(-1), depending on the OCP and type of wine.


英文关键词Gas chromatography-mass spectrometry Solid-phase extraction Organochlorine pesticides in wine
类型Article
语种英语
国家Spain
收录类别SCI-E
WOS记录号WOS:000277595400021
WOS关键词SOLID-PHASE EXTRACTION ; CAPILLARY GAS-CHROMATOGRAPHY ; MASS-SPECTROMETRIC DETECTION ; RED WINES ; RESIDUES ; PORTUGAL ; ORGANOPHOSPHORUS ; LIQUID ; HONEY
WOS类目Biochemical Research Methods ; Chemistry, Analytical
WOS研究方向Biochemistry & Molecular Biology ; Chemistry
资源类型期刊论文
条目标识符http://119.78.100.177/qdio/handle/2XILL650/163675
作者单位1.Univ Cordoba, Dept Analyt Chem, E-14071 Cordoba, Spain;
2.SANYRES XXI, Cordoba 14012, Spain
推荐引用方式
GB/T 7714
Antonio Perez-Serradilla, Jose,Maria Mata-Granados, Jose,Luque de Castro, Maria Dolores. Low-Level Determination of Organochlorine Pesticides in Wines by Automatic Preconcentration and GC-MS-MS Detection[J],2010,71(9-10):899-905.
APA Antonio Perez-Serradilla, Jose,Maria Mata-Granados, Jose,&Luque de Castro, Maria Dolores.(2010).Low-Level Determination of Organochlorine Pesticides in Wines by Automatic Preconcentration and GC-MS-MS Detection.CHROMATOGRAPHIA,71(9-10),899-905.
MLA Antonio Perez-Serradilla, Jose,et al."Low-Level Determination of Organochlorine Pesticides in Wines by Automatic Preconcentration and GC-MS-MS Detection".CHROMATOGRAPHIA 71.9-10(2010):899-905.
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