Knowledge Resource Center for Ecological Environment in Arid Area
DOI | 10.1365/s10337-010-1575-0 |
Low-Level Determination of Organochlorine Pesticides in Wines by Automatic Preconcentration and GC-MS-MS Detection | |
Antonio Perez-Serradilla, Jose1; Maria Mata-Granados, Jose1,2; Luque de Castro, Maria Dolores1 | |
通讯作者 | Luque de Castro, Maria Dolores |
来源期刊 | CHROMATOGRAPHIA
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ISSN | 0009-5893 |
出版年 | 2010 |
卷号 | 71期号:9-10页码:899-905 |
英文摘要 | Solid-phase extraction using automated equipment has been applied to different types of wine (red, white, sparkling and ros,) spiked with 16 organochlorine pesticides (OCPs) for their preconcentration. PRPS, Oasis HLB, Hysphere Resin SH, Resin GP, C8 and C18 sorbent cartridges were tested. The separation-detection step was carried out by gas chromatography-tandem mass spectrometry. Changes in both the volume flushed through the sorbent (ranging between 25 and 100 mL) and the volume injected into the chromatograph (1 or 10 mu L) allow the detection limits of the method to be adapted to the analytes contents in the target samples. Preconcentrating 100 mL of wine and injecting into the chromatrograph 10 mu L of extract, limits of detection obtained for the OPCs range between 1.7 and 9.7 ng L(-1), depending on the OCP and type of wine. |
英文关键词 | Gas chromatography-mass spectrometry Solid-phase extraction Organochlorine pesticides in wine |
类型 | Article |
语种 | 英语 |
国家 | Spain |
收录类别 | SCI-E |
WOS记录号 | WOS:000277595400021 |
WOS关键词 | SOLID-PHASE EXTRACTION ; CAPILLARY GAS-CHROMATOGRAPHY ; MASS-SPECTROMETRIC DETECTION ; RED WINES ; RESIDUES ; PORTUGAL ; ORGANOPHOSPHORUS ; LIQUID ; HONEY |
WOS类目 | Biochemical Research Methods ; Chemistry, Analytical |
WOS研究方向 | Biochemistry & Molecular Biology ; Chemistry |
资源类型 | 期刊论文 |
条目标识符 | http://119.78.100.177/qdio/handle/2XILL650/163675 |
作者单位 | 1.Univ Cordoba, Dept Analyt Chem, E-14071 Cordoba, Spain; 2.SANYRES XXI, Cordoba 14012, Spain |
推荐引用方式 GB/T 7714 | Antonio Perez-Serradilla, Jose,Maria Mata-Granados, Jose,Luque de Castro, Maria Dolores. Low-Level Determination of Organochlorine Pesticides in Wines by Automatic Preconcentration and GC-MS-MS Detection[J],2010,71(9-10):899-905. |
APA | Antonio Perez-Serradilla, Jose,Maria Mata-Granados, Jose,&Luque de Castro, Maria Dolores.(2010).Low-Level Determination of Organochlorine Pesticides in Wines by Automatic Preconcentration and GC-MS-MS Detection.CHROMATOGRAPHIA,71(9-10),899-905. |
MLA | Antonio Perez-Serradilla, Jose,et al."Low-Level Determination of Organochlorine Pesticides in Wines by Automatic Preconcentration and GC-MS-MS Detection".CHROMATOGRAPHIA 71.9-10(2010):899-905. |
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