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CONFIRMATORY METHOD FOR DETERMINATION OF COCCIDIOSTATS IN EGGS
Olejnik, Malgorzata; Szprengier-Juszkiewicz, Teresa; Jedziniak, Piotr
通讯作者Olejnik, Malgorzata
来源期刊BULLETIN OF THE VETERINARY INSTITUTE IN PULAWY
ISSN0042-4870
出版年2010
卷号54期号:3页码:327-333
英文摘要

The method for confirmatory analysis of clazuril, decoquinate, diclazuril, halofuginone, lasalocid, maduramicin, monensin, narasin, nicarbazin, robenidine, salinomycin, and semduramicin in eggs has been developed and validated. The samples were extracted with acetonitrile, purified on Oasis HLB SPE columns and analysed by liquid chromatography coupled with tandem mass spectrometry. The validation, performed according to the EU requirements, proved that the method enables the confirmation of coccidiostats in eggs at the levels required in the official control of residues (CC alpha in the range of 2.92-178 mu g/kg, depending on the coccidiostat). The within-laboratory reproducibility (CV in the range of 6.1-29.3%) is also acceptable. The method was successfully verified in the proficiency test and implemented in the national residue control plan.


英文关键词eggs coccidiostats residues mass spectrometry
类型Article
语种英语
国家Poland
收录类别SCI-E
WOS记录号WOS:000282420900009
WOS关键词TANDEM MASS-SPECTROMETRY ; LIQUID-CHROMATOGRAPHY ; RESIDUES ; NICARBAZIN ; CHICKEN ; POULTRY ; TISSUES ; MUSCLE ; FEED
资源类型期刊论文
条目标识符http://119.78.100.177/qdio/handle/2XILL650/163581
作者单位Natl Inst Vet Res, Dept Pharmacol & Toxicol, PL-24100 Pulawy, Poland
推荐引用方式
GB/T 7714
Olejnik, Malgorzata,Szprengier-Juszkiewicz, Teresa,Jedziniak, Piotr. CONFIRMATORY METHOD FOR DETERMINATION OF COCCIDIOSTATS IN EGGS[J],2010,54(3):327-333.
APA Olejnik, Malgorzata,Szprengier-Juszkiewicz, Teresa,&Jedziniak, Piotr.(2010).CONFIRMATORY METHOD FOR DETERMINATION OF COCCIDIOSTATS IN EGGS.BULLETIN OF THE VETERINARY INSTITUTE IN PULAWY,54(3),327-333.
MLA Olejnik, Malgorzata,et al."CONFIRMATORY METHOD FOR DETERMINATION OF COCCIDIOSTATS IN EGGS".BULLETIN OF THE VETERINARY INSTITUTE IN PULAWY 54.3(2010):327-333.
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