Knowledge Resource Center for Ecological Environment in Arid Area
CONFIRMATORY METHOD FOR DETERMINATION OF COCCIDIOSTATS IN EGGS | |
Olejnik, Malgorzata; Szprengier-Juszkiewicz, Teresa; Jedziniak, Piotr | |
通讯作者 | Olejnik, Malgorzata |
来源期刊 | BULLETIN OF THE VETERINARY INSTITUTE IN PULAWY
![]() |
ISSN | 0042-4870 |
出版年 | 2010 |
卷号 | 54期号:3页码:327-333 |
英文摘要 | The method for confirmatory analysis of clazuril, decoquinate, diclazuril, halofuginone, lasalocid, maduramicin, monensin, narasin, nicarbazin, robenidine, salinomycin, and semduramicin in eggs has been developed and validated. The samples were extracted with acetonitrile, purified on Oasis HLB SPE columns and analysed by liquid chromatography coupled with tandem mass spectrometry. The validation, performed according to the EU requirements, proved that the method enables the confirmation of coccidiostats in eggs at the levels required in the official control of residues (CC alpha in the range of 2.92-178 mu g/kg, depending on the coccidiostat). The within-laboratory reproducibility (CV in the range of 6.1-29.3%) is also acceptable. The method was successfully verified in the proficiency test and implemented in the national residue control plan. |
英文关键词 | eggs coccidiostats residues mass spectrometry |
类型 | Article |
语种 | 英语 |
国家 | Poland |
收录类别 | SCI-E |
WOS记录号 | WOS:000282420900009 |
WOS关键词 | TANDEM MASS-SPECTROMETRY ; LIQUID-CHROMATOGRAPHY ; RESIDUES ; NICARBAZIN ; CHICKEN ; POULTRY ; TISSUES ; MUSCLE ; FEED |
资源类型 | 期刊论文 |
条目标识符 | http://119.78.100.177/qdio/handle/2XILL650/163581 |
作者单位 | Natl Inst Vet Res, Dept Pharmacol & Toxicol, PL-24100 Pulawy, Poland |
推荐引用方式 GB/T 7714 | Olejnik, Malgorzata,Szprengier-Juszkiewicz, Teresa,Jedziniak, Piotr. CONFIRMATORY METHOD FOR DETERMINATION OF COCCIDIOSTATS IN EGGS[J],2010,54(3):327-333. |
APA | Olejnik, Malgorzata,Szprengier-Juszkiewicz, Teresa,&Jedziniak, Piotr.(2010).CONFIRMATORY METHOD FOR DETERMINATION OF COCCIDIOSTATS IN EGGS.BULLETIN OF THE VETERINARY INSTITUTE IN PULAWY,54(3),327-333. |
MLA | Olejnik, Malgorzata,et al."CONFIRMATORY METHOD FOR DETERMINATION OF COCCIDIOSTATS IN EGGS".BULLETIN OF THE VETERINARY INSTITUTE IN PULAWY 54.3(2010):327-333. |
条目包含的文件 | 条目无相关文件。 |
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。