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DOI	10.1016/j.chroma.2009.04.070
	An analytical method for the determination of perfluorinated compounds in whole blood using acetonitrile and solid phase extraction methods
	Yeung, Leo W. Y.1,2; Taniyasu, Sachi 1; Kannan, Kurunthachalam 3,4; Xu, Della Z. Y.2; Guruge, Keerthi S.5; Lam, Paul K. S.2; Yamashita, Nobuyoshi 1
通讯作者	Yamashita, Nobuyoshi
来源期刊	JOURNAL OF CHROMATOGRAPHY A
ISSN	0021-9673
EISSN	1873-3778
出版年	2009
卷号	1216 期号:25 页码:4950-4956
英文摘要	A method for the analysis of perfluorinated compounds (perfluoroalkyl sulfonates: C4, C6, C8, C10; perfluoroalkyl sulfinates: C6, C8, C10; perfluorooctanesulfonamide, N-ethyl perfluorooctanesulfonamide, N-ethyl perfluorooctanesulfonamidoacetate, perfluorocarboxylates: C4-C14; fluorotelomer carboxylate (7:3, 8:2) in whole blood using acetonitrile and OASIS WAX (R) solid phase extraction (SPE) cartridge was developed. Separation of target compounds in two HPLC columns (ion exchange JJ50-2D and C18 Betasil columns) was examined. Matrix recoveries of the developed methods ranged from 70% to 120%. Separation of possible inferences Such as taurodeoxycholic acid (TDC) was accomplished using an ion exchange JJ50-2D column, and this separation was validated using whole blood of different animals. (C) 2009 Elsevier B.V. All rights reserved.
英文关键词	Whole blood Acetonitrile Solid phase extraction Formic acid Taurodeoxycholic acid Perfluorooctanesulfonate
类型	Article
语种	英语
国家	Japan ; Peoples R China ; USA
收录类别	SCI-E
WOS记录号	WOS:000267086400003
WOS关键词	TANDEM MASS-SPECTROMETRY ; PERFLUOROOCTANE SULFONATE ; ORGANIC FLUORINE ; SOUTH CHINA ; HUMAN SERUM ; SHORT-CHAIN ; ACIDS ; FLUOROCHEMICALS ; MATRICES ; SAMPLES
WOS类目	Biochemical Research Methods ; Chemistry, Analytical
WOS研究方向	Biochemistry & Molecular Biology ; Chemistry
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/161412
作者单位	1.Natl Inst Adv Ind Sci & Technol, Tsukuba, Ibaraki 3058569, Japan; 2.City Univ Hong Kong, Dept Biol & Chem, Kowloon, Hong Kong, Peoples R China; 3.SUNY Albany, Wadsworth Ctr, New York State Dept Hlth, Albany, NY 12201 USA; 4.SUNY Albany, Dept Environm Hlth Sci, Albany, NY 12201 USA; 5.Natl Inst Anim Hlth, Safety Res Team, Tsukuba, Ibaraki 3050856, Japan
推荐引用方式 GB/T 7714	Yeung, Leo W. Y.,Taniyasu, Sachi,Kannan, Kurunthachalam,et al. An analytical method for the determination of perfluorinated compounds in whole blood using acetonitrile and solid phase extraction methods[J],2009,1216(25):4950-4956.
APA	Yeung, Leo W. Y..,Taniyasu, Sachi.,Kannan, Kurunthachalam.,Xu, Della Z. Y..,Guruge, Keerthi S..,...&Yamashita, Nobuyoshi.(2009).An analytical method for the determination of perfluorinated compounds in whole blood using acetonitrile and solid phase extraction methods.JOURNAL OF CHROMATOGRAPHY A,1216(25),4950-4956.
MLA	Yeung, Leo W. Y.,et al."An analytical method for the determination of perfluorinated compounds in whole blood using acetonitrile and solid phase extraction methods".JOURNAL OF CHROMATOGRAPHY A 1216.25(2009):4950-4956.