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A Rapid High Performance Liquid Chromatographic Method for Determination of Tiamulin Residue in Swine Tissues | |
Cheng Lin-Li; Zhang Su-Xia; Shen Jian-Zhong; Wang Zhan-Hui; Li Yan-Shen; Feng Pei-Sheng | |
通讯作者 | Cheng Lin-Li |
来源期刊 | CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
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ISSN | 0253-3820 |
EISSN | 1872-2040 |
出版年 | 2009 |
卷号 | 37期号:5页码:718-720 |
英文摘要 | A rapid method has been developed for the determination of tiamulin (TML) residue in swine tissues by high performance liquid chromatography. The samples were extracted with phosphate buffer-ethyl acetate solution, and then centrifuged by 5000 rpm for 10 min, 0.1% fartrate solution was added in the supernatant obtained with liguid-liquid-liquid extraction, and the organic phase was eveporated. After fats having been removed with hexan, further purification was performed with Oasis HLB solid phase extraction column. The TML residue was determined by HPLC with a mobile phase of acetonitrile-0.0125% acetic acid(42:58, V/V) and UV detection at 210 nm. The average recovery rates of TML in pork and swine liver were in the range of 80.1% - 92.7% when spiked 25 - 500 mu g/kg. The RSD ranged from 2.0% to 13.9%. The detection limits were 5 mu g/kg and 8 mu g/kg for pork and swine liver, respectively. |
英文关键词 | Tiamulin pork swine liver high performance liquid chromatography |
类型 | Article |
语种 | 中文 |
国家 | Peoples R China |
收录类别 | SCI-E |
WOS记录号 | WOS:000266385500019 |
WOS关键词 | MEAT |
WOS类目 | Chemistry, Analytical |
WOS研究方向 | Chemistry |
来源机构 | 中国农业大学 |
资源类型 | 期刊论文 |
条目标识符 | http://119.78.100.177/qdio/handle/2XILL650/160157 |
作者单位 | China Agr Univ, Coll Vet Med, Beijing 100193, Peoples R China |
推荐引用方式 GB/T 7714 | Cheng Lin-Li,Zhang Su-Xia,Shen Jian-Zhong,et al. A Rapid High Performance Liquid Chromatographic Method for Determination of Tiamulin Residue in Swine Tissues[J]. 中国农业大学,2009,37(5):718-720. |
APA | Cheng Lin-Li,Zhang Su-Xia,Shen Jian-Zhong,Wang Zhan-Hui,Li Yan-Shen,&Feng Pei-Sheng.(2009).A Rapid High Performance Liquid Chromatographic Method for Determination of Tiamulin Residue in Swine Tissues.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,37(5),718-720. |
MLA | Cheng Lin-Li,et al."A Rapid High Performance Liquid Chromatographic Method for Determination of Tiamulin Residue in Swine Tissues".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 37.5(2009):718-720. |
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