Arid
A Rapid High Performance Liquid Chromatographic Method for Determination of Tiamulin Residue in Swine Tissues
Cheng Lin-Li; Zhang Su-Xia; Shen Jian-Zhong; Wang Zhan-Hui; Li Yan-Shen; Feng Pei-Sheng
通讯作者Cheng Lin-Li
来源期刊CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
ISSN0253-3820
EISSN1872-2040
出版年2009
卷号37期号:5页码:718-720
英文摘要

A rapid method has been developed for the determination of tiamulin (TML) residue in swine tissues by high performance liquid chromatography. The samples were extracted with phosphate buffer-ethyl acetate solution, and then centrifuged by 5000 rpm for 10 min, 0.1% fartrate solution was added in the supernatant obtained with liguid-liquid-liquid extraction, and the organic phase was eveporated. After fats having been removed with hexan, further purification was performed with Oasis HLB solid phase extraction column. The TML residue was determined by HPLC with a mobile phase of acetonitrile-0.0125% acetic acid(42:58, V/V) and UV detection at 210 nm. The average recovery rates of TML in pork and swine liver were in the range of 80.1% - 92.7% when spiked 25 - 500 mu g/kg. The RSD ranged from 2.0% to 13.9%. The detection limits were 5 mu g/kg and 8 mu g/kg for pork and swine liver, respectively.


英文关键词Tiamulin pork swine liver high performance liquid chromatography
类型Article
语种中文
国家Peoples R China
收录类别SCI-E
WOS记录号WOS:000266385500019
WOS关键词MEAT
WOS类目Chemistry, Analytical
WOS研究方向Chemistry
来源机构中国农业大学
资源类型期刊论文
条目标识符http://119.78.100.177/qdio/handle/2XILL650/160157
作者单位China Agr Univ, Coll Vet Med, Beijing 100193, Peoples R China
推荐引用方式
GB/T 7714
Cheng Lin-Li,Zhang Su-Xia,Shen Jian-Zhong,et al. A Rapid High Performance Liquid Chromatographic Method for Determination of Tiamulin Residue in Swine Tissues[J]. 中国农业大学,2009,37(5):718-720.
APA Cheng Lin-Li,Zhang Su-Xia,Shen Jian-Zhong,Wang Zhan-Hui,Li Yan-Shen,&Feng Pei-Sheng.(2009).A Rapid High Performance Liquid Chromatographic Method for Determination of Tiamulin Residue in Swine Tissues.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,37(5),718-720.
MLA Cheng Lin-Li,et al."A Rapid High Performance Liquid Chromatographic Method for Determination of Tiamulin Residue in Swine Tissues".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 37.5(2009):718-720.
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