干旱区生态环境知识资源中心(Arid): Quantification of low levels of organochlorine pesticides using small volumes (<= 100 mu l) of plasma of wild birds through gas chromatography negative chemical ionization mass spectrometry

Arid

DOI	10.1016/j.envpol.2006.11.018
	Quantification of low levels of organochlorine pesticides using small volumes (<= 100 mu l) of plasma of wild birds through gas chromatography negative chemical ionization mass spectrometry
	Rivera-Rodriguez, Laura B.; Rodriguez-Estrella, Ricardo; Ellington, James Jackson; Evans, John J.
通讯作者	Rivera-Rodriguez, Laura B.
来源期刊	ENVIRONMENTAL POLLUTION
ISSN	0269-7491
EISSN	1873-6424
出版年	2007
卷号	148 期号:2 页码:654-662
英文摘要	A solid phase extraction and gas chromatography with negative chemical ionization mass spectrometry in scan mode (GC-NCI-MS) method was developed to identify and quantify for the first time low levels of organochlorine pesticides (OCs) in plasma samples of less than 100 mu l from wild birds. The method detection limits ranged from 0.012 to 0.102 pg/mu l and the method reporting limit from 0.036 to 0.307 pg/mu l for alpha, gamma, beta and delta-hexachlorocyclohexane (HCH), heptachlor, aldrin, heptachlor epoxide, endosulfan I, 1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene (p,p’-DDE), dieldrin, endrin, endosulfan-II, endrin-aldehyde and endosulfan-sulfate. Pesticide levels in small serum samples from individual Falco sparverius, Sturnella neglecta, Mimus polyglottos and Columbina passerina were quantified. Concentrations ranged from not detected (n/d) to 204.9 pg/mu l for some OC pesticides. All levels in the food web in and around cultivated areas showed the presence of pesticides notwithstanding the small areas for agriculture existing in the desert of Baja California peninsula. (c) 2006 Elsevier Ltd. All rights reserved.
英文关键词	avian plasma SPE HLB-urea extraction GC-NCI-MS organochlorine Baja California sur
类型	Article
语种	英语
国家	Mexico ; USA
收录类别	SCI-E
WOS记录号	WOS:000247541100032
WOS关键词	SOLID-PHASE EXTRACTION ; POLYCHLORINATED-BIPHENYLS ; GREAT-LAKES ; HUMAN SERUM ; CHLORINATED PESTICIDES ; NORTH PACIFIC ; CASPIAN TERNS ; PCBS ; CONTAMINANTS ; PRODUCTIVITY
WOS类目	Environmental Sciences
WOS研究方向	Environmental Sciences & Ecology
资源类型	期刊论文
条目标识符	http://119.78.100.177/qdio/handle/2XILL650/154138
作者单位	(1)Ctr Invest Biol Noroeste, SC Environm Planning & Conservat Program, La Paz 23090, Baja California, Mexico;(2)US EPA, Natl Exposure Res Lab, Athens, GA 30605 USA
推荐引用方式 GB/T 7714	Rivera-Rodriguez, Laura B.,Rodriguez-Estrella, Ricardo,Ellington, James Jackson,et al. Quantification of low levels of organochlorine pesticides using small volumes (<= 100 mu l) of plasma of wild birds through gas chromatography negative chemical ionization mass spectrometry[J],2007,148(2):654-662.
APA	Rivera-Rodriguez, Laura B.,Rodriguez-Estrella, Ricardo,Ellington, James Jackson,&Evans, John J..(2007).Quantification of low levels of organochlorine pesticides using small volumes (<= 100 mu l) of plasma of wild birds through gas chromatography negative chemical ionization mass spectrometry.ENVIRONMENTAL POLLUTION,148(2),654-662.
MLA	Rivera-Rodriguez, Laura B.,et al."Quantification of low levels of organochlorine pesticides using small volumes (<= 100 mu l) of plasma of wild birds through gas chromatography negative chemical ionization mass spectrometry".ENVIRONMENTAL POLLUTION 148.2(2007):654-662.